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The establishment of EVISA is funded by the EU through the Fifth Framework Programme (G7RT- CT- 2002- 05112).
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Material Database:
INCT-TL-1 Tea Leaves
Type
Certified reference material
Producer
Institute of Nuclear Chemistry and Technology (INCT/ICHTJ)
Status
Available
Material
Powder
Reference
INCT-TL-1
Catalog (Web)
https://www.lgcstandards.com/GB/en/Tea-leaves-Trace-elemen
ts/p/IC-INCT-TL-1
Description
The material was prepared from black tea, usually packed in tea bags. Tea leaves collected and processed in Argentina were ground and sieved. All precautions were taken to avoid contamination of the material with metals. The next step was homogenization by mixing in a plastic drum. After preliminary homogeneity checking by X-ray fluorescence, the material was distributed into PP bottles and final homogeneity testing was performed by neutron activation analysis determining Br, Ce, Co, Cr, Cs, Fe, K, La, Mn, Na, Rb, Sc and Sm in subsamples (Fisher’s test). Good homogeneity of INCT-TL-1 at least for sample weight of 5 mg was confirmed. Long-term stability has been assured by sterilization of the whole lot of the material by electron beam radiation and is being monitored during storage. Certification of the candidate reference material was done on the basis of world-wide interlaboratory comparison exercise in which 109 laboratories from 19 countries using various analytical methods, participated. Data evaluation was performed using the software package ACQS-1. Several criteria were employed to decide whether the overall mean can be given the status of recommended (certified) or information value. The validity of certified values was confirmed for several elements using definitive methods developed in this Laboratory.
Package
50 g
Parameter
Analyte
Aluminum
Specification
total aluminum
Parameter
Certified value
Unit
wt, %
Result
0.229 ± 0.028
Analyte
Arsenic
Specification
total arsenic
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.106 ± 0.021
Analyte
Barium
Specification
total barium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
43.2 ± 3.9
Analyte
Bromine
Specification
total bromine
Parameter
Certified value
Unit
mg/kg (ppm)
Result
12.3 ± 1.0
Analyte
Cadmium
Specification
total cadmium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.030 ± 0.004
Analyte
Calcium
Specification
total calcium
Parameter
Certified value
Unit
wt, %
Result
0.582 ± 0.052
Analyte
Cesium
Specification
total cesium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
3.61 ± 0.37
Analyte
Chlorine
Specification
total chlorine
Parameter
Certified value
Unit
mg/kg (ppm)
Result
573 ± 48
Analyte
Chromium
Specification
total chromium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
1.91 ± 0.22
Analyte
Cobalt
Specification
total cobalt
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.387 ± 0.042
Analyte
Copper
Specification
total copper
Parameter
Certified value
Unit
mg/kg (ppm)
Result
20.4 ± 1.5
Analyte
Europium
Specification
total europium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.050 ± 0.009
Analyte
Lanthanum
Specification
total lanthanum
Parameter
Certified value
Unit
mg/kg (ppm)
Result
1.00 ± 0.07
Analyte
Lead
Specification
total lead
Parameter
Certified value
Unit
mg/kg (ppm)
Result
1.78 ± 0.24
Analyte
Lutetium
Specification
total lutetium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.017 ± 0.002
Analyte
Magnesium
Specification
total magnesium
Parameter
Certified value
Unit
wt, %
Result
0.224 ± 0.017
Analyte
Manganese
Specification
total manganese
Parameter
Certified value
Unit
wt, %
Result
0.157 ± 0.011
Analyte
Mercury
Specification
total mercury
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.005 ± 0.0007
Analyte
Nickel
Specification
total nickel
Parameter
Certified value
Unit
mg/kg (ppm)
Result
6.12 ± 0.52
Analyte
Potassium
Specification
total potassium
Parameter
Certified value
Unit
wt, %
Result
1.70 ± 0.12
Analyte
Rubidium
Specification
total rubidium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
81.5 ± 6.5
Analyte
Samarium
Specification
total samarium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.177 ± 0.022
Analyte
Scandium
Specification
total scandium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.266 ± 0.024
Analyte
Sodium
Specification
total sodium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
24.7 ± 3.2
Analyte
Strontium
Specification
total strontium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
20.8 ± 1.7
Analyte
Sulfur
Specification
total sulfur (total sulphur)
Parameter
Certified value
Unit
wt, %
Result
0.247 ± 0.025
Analyte
Terbium
Specification
Total terbium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.027 ± 0.002
Analyte
Thallium
Specification
total thallium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.063 ± 0.005
Analyte
Thorium
Specification
total thorium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.034 ± 0.005
Analyte
Vanadium
Specification
total vanadium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
1.97 ± 0.37
Analyte
Ytterbium
Specification
total ytterbium
Parameter
Certified value
Unit
mg/kg (ppm)
Result
0.118 ± 0.013
Analyte
Zinc
Specification
total zinc
Parameter
Certified value
Unit
mg/kg (ppm)
Result
34.7 ± 2.7
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