System specifications
Sample number
80 (with SIL-10A, Rack L)
Mobile phase flow rate
Preparative: 10-30mL/min (Sprit ratio, ESI; 1:99, APCI; 1:29)
Analytical: 1-3mL/min (Sprit ratio, ESI; 1:9, APCI; 1:2)
Analog output
Number of channel: 2 channels
Output signal type:
TIC, MIC, MC, SIM
Fraction collector control
Peak slope fraction, Level fraction, Manual fraction
Fraction collector time program
Possible
Fraction error check
Done by set retention time. In case error occurs, schedule stops.
Mass Spectrometer Specifications
Mass range
m/z 10-1500 (type: S)
m/z 10-2000 (Type: H)
Resolution
R=2M (half width)
Sensitivity
ESI: S/N>80, 50pg of Papaverine, flow injection, SIM mode
APCI: S/N>80, 50pg of Papaverine, flow injection, SIM mode
Max. scan speed
6,000u/sec. (centroid scan)
4,000u/sec.(profile scan)
When profile scan is executed at 4,000u/sec., maximum measurement time is reduced.
Interfaces
ESI and APCI
ESI probe
Max. flow rate: 1mL/min
APCI probe
Max. flow rate: 2mL/min
Max. temperature:
500deg.C
CDL (desolvation unit)
Max. temperature: 300deg.C
Analyzer
Detector rods
Hyperbolic quadrulpole rods with pre rods
Detector
Secondary ion multiplier with conversion dynode
Detectable ions
Positive and Negative, selectable
Vacuum system
Main pump
210L/sec Turbo molecular pump and 56L/sec Turbo molecular pump
Fore pump
28m3/hr rotary pump
Software (LCMS solution)
LC control
LC-8A, FCV-12AH, SPD-10AVP, SIL-10A, FRC-10A
Tuning
Autotuning/Manual tuning with standard sample
Vacuum control
Auto start-up, Auto shut-down
Data processing
Display of real time fraction marking on preparative run
TIC chromatogram, display
MC display
Spectrum display
Quantitation from MS data
Peak profile spectrum display
Molecular weight estimation from multiple ion spectrum
Report generation, Fraction marking display
Security
Audit trail
others
