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Peer reviewing - Recommendations to reviewers of analytical chemistry papers

(12.08.2024)


Here are some recommendations for reviewers in this field:

1. Assess the Scientific Rigor
  • Method Validation: Ensure that the methods used are properly validated. Check if the authors have provided sufficient evidence that their analytical methods are accurate, precise, sensitive, and reproducible.
  • Data Quality: Evaluate the quality of the data presented. Look for appropriate controls, replicates, and statistical analyses to support the conclusions.
  • Error Analysis: Assess how well the authors have accounted for potential errors in their measurements and analyses. Verify that they have discussed the limitations and sources of uncertainty in their data.

2. Evaluate the Novelty and Impact
  • Innovation: Consider whether the paper presents a novel approach or significant advancement in the field of analytical chemistry. Determine if the findings contribute new knowledge or a new application of existing methods.
  • Practical Relevance: Assess the practical applicability of the research. Does it address a real-world problem, and could it be implemented in a laboratory or industrial setting?

3. Examine the Clarity and Transparency
  • Methodological Transparency: Ensure that the authors have provided sufficient detail about their experimental procedures so that other researchers could replicate the study. Look for detailed descriptions of materials, instruments, and protocols, including the important parameters.
  • Data Presentation: Check that the data is presented clearly and logically. Figures, tables, and graphs should be easy to understand and directly support the paper's conclusions.
  • Interpretation of Results: Review how well the authors have interpreted their data. Ensure that their conclusions are supported by the data and that they have not overstated their findings.

4. Ensure Correct Use of Acronyms, Abbreviations and Terminology
  • IUPAC Standards: Verify that the authors are using terminology that conforms to IUPAC (International Union of Pure and Applied Chemistry) standards, especially for chemical nomenclature, units of measurement, and analytical methods.
  • Analytical Techniques: Ensure that the names of analytical techniques (e.g., HPLC, GC-MS, NMR) and related terminology are used accurately and consistently throughout the paper.
  • Acronyms and Abbreviations: Ensure that acronyms and abbreviations are defined upon first use and used consistently throughout the paper. Misused or inconsistent abbreviations can lead to misunderstandings.
  • Terminology Consistency: Review the paper for consistent use of terms, particularly when referring to specific chemicals, methods, or instruments. Inconsistent terminology can confuse readers and undermine the clarity of the research.
  • Avoid Jargon: Ensure that the paper avoids unnecessary jargon or overly complex language that might obscure the main findings. The terminology should be appropriate for the intended audience of the journal.

5. Consider Ethical Aspects
  • Ethical Approval: If the research involves human or animal subjects, verify that the authors have obtained appropriate ethical approvals and have followed relevant guidelines.
  • Conflicts of Interest: Be alert to potential conflicts of interest that might affect the integrity of the research. This includes financial ties or affiliations that could bias the study.

6. Verify References and Citations
  • Literature Review: Check that the authors have cited relevant literature appropriately. Ensure that they have provided a comprehensive and up-to-date review of the field.
  • Original Work: Verify that the work is original and not a redundant publication of previous research by the same authors.

7. Provide Constructive Feedback
  • Balanced Criticism: Offer constructive criticism that helps the authors improve their work. Be specific about what needs to be improved, and suggest possible solutions or additional experiments if needed.
  • Positivity with Purpose: Acknowledge the strengths of the paper alongside any critiques. Highlighting strong points can help guide authors on what aspects to preserve as they revise.
  • Tone and Professionalism: Maintain a professional and respectful tone, even when pointing out significant flaws or weaknesses in the paper.

8. Adhere to Deadlines and Guidelines
  • Timeliness: Respect the deadlines set by the journal. Providing a timely review helps the editorial process and supports the authors' need for prompt feedback.
  • Journal Standards: Familiarize yourself with the journal's standards and guidelines for reviewers. Ensure your review aligns with the journal's expectations.

9. Engage in Self-Education
  • Stay Informed: Continuously educate yourself on new developments and trends in analytical chemistry. This will improve the quality of your reviews and keep you current with the field.
  • Bias Awareness: Be aware of your own biases, and strive to minimize their impact on your review. Approach each paper with an open mind, focusing on the content rather than the authors or institutions.
By following these recommendations, reviewers can contribute significantly to the advancement of analytical chemistry and help maintain the integrity and quality of published research. The expectations from peer reviewing call for competent and fair reviewers, which have to handle an ever-increasing number of papers timeliness. In principle, all authors submitting papers to peer-reviewed journals have an obligation also to act as reviewers. Requirements for acting as a reviewer are expertise in the topic to be reviewed, adherence to research reporting standards, and having the necessary time to do the review timely. Access to bibliographic databases are recommended to help reviewers draft evidence-based and detailed comments.


Related information on good practice in reviewing

Rebecca Sear: Good Practice in Peer Review

Rosy Hosking (MIT Communication Lab): Peer Review - Best Practices

Rebecca Sear (The Royal Society). Tips for good practice in peer review




Related publications on good practice in reviewing

Oleana Zimba, Armen Yuri Gasparyan, Peer review guidance: a primer for researchers, Reumatologia, 59/1 (2021) 3-8. DOI: 10.5114/reum.2021.102709
Heidi Allen, Alexandra Cury, Thomas Gaston, Chris Graf, Hannah Wakley, and Michael Willis, What does better peer review look like? Underlying principles and recommendations for better practice, Learned Publishing, 32 (2019) 163–175. DOI: 10.1002/leap.1222
Irene Hames, Peer review golden rules and good practice checklist, Sci. edit., 3/1 (2016) 36-42. DOI: 10.6087/kcse.61
Robert J. DiDomenico, William L. Baker, Stuart T. Haines, Improving peer review: What reviewers can do, Am. J. Health Syst. Pharm., 74 (2017) 2080-2084. DOI 10.2146/ajhp170190
Calvin Chong, Reviewing/editing a manuscript for scientific publication, Can. J. Plant Sci., 78/3 (1998) 377-382. DOI: 10.4141/p97-112


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